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Beilstein J. Org. Chem. 2018, 14, 688–696, doi:10.3762/bjoc.14.57
Graphical Abstract
Figure 1: Solution-based Wittig reaction mechanism.
Figure 2: 1H NMR spectra of stilbene mixture (a) and benzyl benzoate (b).
Scheme 1: Possible mechanism of benzyl benzoate formation.
Scheme 2: A possible mechanistic explanation for the E selectivity.
Scheme 3: Ball-milled Wittig reaction using excess benzaldehyde.
Figure 3: Comparison of solution based Wittig reaction (a) with polymer-supported mechanochemical Wittig reac...
Scheme 4: Stepwise ball-milled Wittig reaction with ethanol as the LAG solvent.
Scheme 5: Stepwise ball-milled Wittig reaction with ethanol evaporation between the steps.